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If you are given the lengths of 3 sides of a right triangle...
SinΘ = opp/hyp
This means that if you divide the two lengths that correspond to the side opposite the angle you are looking for and the hypotenuse the answer will be sinΘ. You can then take the inverse sin to solve for Θ.
You can also use
cosΘ = adj/hyp which is the adjacent side to the angle you are looking for and the hypotenuse
tanΘ = opp/adj which is the opposite divided by the adjacent side
Don't forget to take the inverse function to solve for theta.
As rudi_in said, the info he gave is for a right triangle, i.e. one with one angle = 90degrees.
If the triangle is not a right triangle things get much more complex. The info at http://en.wikipedia.org/wiki/Triangle is enough to figure it out. If you need someone to give assistance let us know.